Cyanamide → N-cyano-3-(4-dimethylaminomethyl-2-pyridylmethylthio)propionamidine

HRID 482659ノート

反応式

HRID 482659 の反応式
CO[C:3](=[NH:18])[CH2:4][CH2:5][S:6][CH2:7][C:8]1[CH:13]=[C:12]([CH2:14][N:15]([CH3:17])[CH3:16])[CH:11]=[CH:10][N:9]=1.[N:19]#[C:20][NH2:21]>CO>[C:20]([NH:21][C:3](=[NH:18])[CH2:4][CH2:5][S:6][CH2:7][C:8]1[CH:13]=[C:12]([CH2:14][N:15]([CH3:17])[CH3:16])[CH:11]=[CH:10][N:9]=1)#[N:19]

参加物

4

反応物 2

HCID 9864CyanamideHCID 19870407Methyl 3-(4-dimethylaminomethyl-2-pyridylmethylthio)propionimidate

生成物 1

HCID 178483279N-cyano-3-(4-dimethylaminomethyl-2-pyridylmethylthio)propionamidine

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

Methyl-3-(4-dimethylaminomethyl-2-pyridylmethylthio)propionimidate is added to a methanol solution of cyanamide. After standing overnight N-cyano-3-(4-dimethylaminomethyl-2-pyridylmethylthio)propionamidine is obtained.

出典と根拠

ORDレコード
ord-1514937795be45a2acd7e1f69636e066
出典データセット
uspto-grants-1986_03
特許番号
US04574126

反応ノート

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