反応式
CS[C:3]1[S:4][CH2:5][CH2:6][N:7]=1.Cl.[Cl:9][C:10]1[C:11]([NH:17][NH2:18])=[C:12]([CH3:16])[CH:13]=[CH:14][CH:15]=1>C(O)(C)C>[Cl:9][C:10]1[C:11]([NH:17][NH:18][C:3]2[S:4][CH2:5][CH2:6][N:7]=2)=[C:12]([CH3:16])[CH:13]=[CH:14][CH:15]=1参加物
4
実験手順
A solution of 11.2 g (5% excess) of 2-methylthio-2-thiazoline in 20 ml of isopropanol was added slowly in the course of 30 minutes to a suspension, which was stirred under reflux, of 15.5 g (0.08 mol) of 3-chloro-2-tolyl-hydrazine hydrochloride in 100 ml of isopropanol.
出典と根拠
- ORDレコード
- ord-2ca251c893084a03b38c979895c8ff64
- 出典データセット
- uspto-grants-1986_03
- 特許番号
- US04575501
関連ノート
読み込み中…