化工社化工社 化学情報印刷レポート · 研究参考用
Ethylenediamine → (9-Chloro-1,2,3,4-tetrahydrobenzo[e][1,4]diazepin-5-ylidenemethyl)phosphonic acid diethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethylenediamine | HCID 3301 | — |
| 反応物 | N-Methylethylenediamine | HCID 8014 | — |
| 反応物 | 3-Chloro-2-fluorobenzoic acid | HCID 302931 | — |
| 反応物 | (1-Methyl-1,2,3,4-tetrahydrobenzo[e][1,4]diazepin-5-ylidenemethyl)phosphonic acid diethyl ester | HCID 72957243 | — |
| 生成物 | (9-Chloro-1,2,3,4-tetrahydrobenzo[e][1,4]diazepin-5-ylidenemethyl)phosphonic acid diethyl ester | HCID 86585810 | — |
反応手順
(9-chloro-1,2,3,4-tetrahydrobenzo[e][1,4]diazepin-5-ylidenemethyl)phosphonic acid diethyl ester was prepared in an analogous fashion to (1-methyl-1,2,3,4-tetrahydrobenzo[e][1,4]diazepin-5-ylidenemethyl)phosphonic acid diethyl ester, prepared in Example 1, by replacing 2-fluorobenzoic acid with 2-fluoro-3-chlorobenzoic acid and N-methylethylenediamine with ethylenediamine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06703387B2 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-156eba81e47e464d806a53a6449d9179 |
| 出典メモ | uspto-grants-2004_03 |