Potassium Carbonate → HCID 178487441、化合物

反応式

Cl.[CH3:2][O:3][C:4]1[CH:13]=[C:12]2[C:7]([CH:8]=[CH:9][CH:10]=[C:11]2[CH2:14][CH2:15][NH2:16])=[CH:6][CH:5]=1.C(=O)([O-])[O-].[K+].[K+].Cl.[NH:24]1[CH:28]=[C:27]([CH2:29][C:30](Cl)=[O:31])[N:26]=[CH:25]1>C(Cl)(Cl)Cl.O>[CH3:2][O:3][C:4]1[CH:13]=[C:12]2[C:7]([CH:8]=[CH:9][CH:10]=[C:11]2[CH2:14][CH2:15][NH:16][C:30](=[O:31])[CH2:29][C:27]2[N:26]=[CH:25][NH:24][CH:28]=2)=[CH:6][CH:5]=1

参加物

実験手順

0.01 mol of 2-(7-methoxynaphth-1-yl)ethylamine hydrochloride is dissolved in 60 ml of a chloroform/water mixture, and 0.025 mol of potassium carbonate is added under magnetic agitation. The mixture is cooled, and 0.012 mol of 4-imidazoleacetyl chloride hydrochloride is added dropwise. The agitation is maintained for 30 minutes at room temperature and the chloroform phase is evaporated to dryness. The residue is then recrystallized.