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Ethyl 1-(p-chlorobenzyl)-5-chloro-3-thiophenylindole-2-carboxylate → 1-(p Chlorobenzyl)-5-chloro-3-thiophenylindole-2-carboxylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 1-(p-chlorobenzyl)-5-chloro-3-thiophenylindole-2-carboxylate | HCID 67855865 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 1-(p Chlorobenzyl)-5-chloro-3-thiophenylindole-2-carboxylic acid | HCID 23200931 | — |
反応手順
Following the procedure of Preparation 6, but using ethyl 1-(p-chlorobenzyl)-5-chloro-3-thiophenylindole-2-carboxylate from Example 1 as the starting material and tetrahydrofuran as the solvent, the title compound was prepared, mp 185°-188° (dec.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05225421 |
| 出典データセット | uspto-grants-1993_07 |
| ORD ID | ord-0e7fc3adaaa749b5ba36e059b32fa6e0 |
| 出典メモ | uspto-grants-1993_07 |