関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Dichlorodifluoromethane | HCID 6391 | — |
| 反応物 | 1-Bromo-1,2,2-trifluoroethene | HCID 11730 | — |
| 反応物 | Bis(fluoroxy)perfluoromethane | HCID 140054 | — |
| 溶媒 | Nitrogen | HCID 947 | — |
| 生成物 | 4-Bromo-2,2,4,5,5-pentafluoro-1,3-dioxolane | HCID 19745410 | — |
反応手順
Into a multineck glass reactor equipped with: magnetic entrainment mechanical stirrer, reflux cooler, thermocouple, inner plunging pipes for introducing the reagents, and maintained at a temperature of -70° C., there were simultaneously fed--after having introduced 75 ml of dichlorodifluoromethane--0.75 l of bis(fluoroxy)difluoromethane at a flowrate of 0.375 l/h diluted with N2 (0.5 l/h) and bromotrifluoroethylene (5.4 g/h) for 2 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05225576 |
|---|
| 出典データセット | uspto-grants-1993_07 |
|---|
| ORD ID | ord-6836a1b108ea495ebd618e95c9b17ff5 |
|---|
| 出典メモ | uspto-grants-1993_07 |
|---|
