関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Tetrafluoroethylene | HCID 8301 | — |
| 反応物 | Bis(fluoroxy)perfluoromethane | HCID 140054 | — |
| 溶媒 | Nitrogen | HCID 947 | — |
| 生成物 | 2,2,4,4,5,5-Hexafluoro-1,3-dioxolane | HCID 23234846 | — |
反応手順
Into a multineck glass reactor equipped with: magnetic entrainment mechanical stirrer, reflux cooler, thermocouple, inner plunging pipes for introducing the reagents, and maintained at a temperature of -80° C., there were simultaneously fed-after having introduced 75 ml of FC 75-0.5 l of bis(fluoroxy)difluoromethane at a flowrate of 0.3 l/h diluted with N2 (0.5 l/h) and 5.0 g of tetrafluoroethylene (3.0 g/h).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05225576 |
|---|
| 出典データセット | uspto-grants-1993_07 |
|---|
| ORD ID | ord-7e4d1cab83d041a3b4ef3f0f9bbd5e9f |
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| 出典メモ | uspto-grants-1993_07 |
|---|
