化工社化工社 化学情報印刷レポート · 研究参考用
Aluminum nitrate nonahydrate → Dialuminium cobalt tetraoxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aluminum nitrate nonahydrate | HCID 24567 | — |
| 反応物 | Cobaltous nitrate hexahydrate | HCID 24821 | — |
| 反応物 | Ammonium Carbonate | HCID 517111 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Dialuminium cobalt tetraoxide | HCID 159384 | — |
反応手順
In 300 ml of pure water were dissolved 29 g of cobalt nitrate hexahydrate and 75 g of aluminum nitrate nonahydrate. A solution of 38.4 g of ammonium carbonate dissolved in 100 ml of pure water was gradually added thereto with stirring to form a gel-form precipitate. The precipitate was washed with pure water three times, dried at 100° C. overnight and calcined at 600° C. in an air stream. The calcined material was then calcined at 800° C. in a muffle furnace for 3 hours to a cobalt aluminate catalyst having a blue color.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05227145 |
| 出典データセット | uspto-grants-1993_07 |
| ORD ID | ord-d755ad4082d34d449f7b2c97f1c17329 |
| 出典メモ | uspto-grants-1993_07 |