関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Perfluoropropionyl fluoride | HCID 67912 | — |
| 反応物 | Potassium Fluoride | HCID 522689 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | 1,1,1,3,3,4,4,4-Octafluoro-2-(trifluoromethyl)-2-butanol | HCID 160813 | — |
反応手順
By operating as in the above examples, 0.26 g of KF (4.5 mmol) was charged to the reactor, and then 4.0 ml of anhydrous acetonitrile was injected through the pierceable cap; the whole was then cooled down to -196° C. with the residual air being evacuated; then, 2.0 mmol of pentafluoropropionyl fluoride
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US05227539 |
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| 出典データセット | uspto-grants-1993_07 |
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| ORD ID | ord-26b6efaca80344a497d3f837a6d8c214 |
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| 出典メモ | uspto-grants-1993_07 |
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