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HRID 483915作成日:2026年10月27日

Perfluoropropionyl fluoride → 1,1,1,3,3,4,4,4-Octafluoro-2-(trifluoromethyl)-2-butanol

https://huagongshe.com/reaction/483915

反応式

関与物質

役割名称HCID仕込み量
反応物Perfluoropropionyl fluorideHCID 67912—
反応物Potassium FluorideHCID 522689—
溶媒AcetonitrileHCID 6342—
生成物1,1,1,3,3,4,4,4-Octafluoro-2-(trifluoromethyl)-2-butanolHCID 160813—

反応条件

温度-196 °C

反応手順

By operating as in the above examples, 0.26 g of KF (4.5 mmol) was charged to the reactor, and then 4.0 ml of anhydrous acetonitrile was injected through the pierceable cap; the whole was then cooled down to -196° C. with the residual air being evacuated; then, 2.0 mmol of pentafluoropropionyl fluoride

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05227539
出典データセットuspto-grants-1993_07
ORD IDord-26b6efaca80344a497d3f837a6d8c214
出典メモuspto-grants-1993_07