Formamide → HCID 178435036、化合物

HRID 48416

反応式

HRID 48416 の反応式
[NH2:1][C:2]1[S:3][C:4]([CH3:13])=[C:5]([CH3:12])[C:6]=1[C:7](OCC)=[O:8].[CH:14]([NH2:16])=O>>[OH:8][C:7]1[C:6]2[C:5]([CH3:12])=[C:4]([CH3:13])[S:3][C:2]=2[N:1]=[CH:14][N:16]=1

参加物

3

実験手順

Using ethyl 2-amino-4,5-dimethylthiophene-3-carboxylate (500 mg, 2.5 mmol) and formamide (5 ml), a similar procedure to a) in Production Example 208 was carried out to obtain 4-hydroxy-5,6-dimethylthieno[2,3-d]pyrimidine (380 mg, 2.1 mmol) having the following physical properties:

出典と根拠

ORDレコード
ord-46f90a519b5943e88f8d76ee4b2208df
出典データセット
uspto-grants-2004_03
特許番号
US06703421B1

関連ノート

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