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2-Aminoindane → 6-(2-Indanylamino)purine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Aminoindane | HCID 76310 | — |
| 反応物 | 6-Chloropurine | HCID 5359277 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 6-(2-Indanylamino)purine | HCID 22719588 | 40% |
反応手順
Using 6-chloropurine (150 mg, 1.0 mmol), 2-aminoindan (200 mg, 1.5 mmol), and ethanol (6 ml), a similar procedure to Production Example 190 was carried out. The precipitate obtained was crystallized from ethanol to obtain the title compound (100 mg, 0.40 mmol) having the following physical properties:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06703421B1 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-d42bfccd9ff1439ea1d53148c4cc039d |
| 出典メモ | uspto-grants-2004_03 |