HCID 178449946、化合物 → HCID 178449950、化合物

HRID 48452ノート

反応式

HRID 48452 の反応式
Cl.[C:2]([NH2:7])(=[O:6])[C:3]([CH3:5])=[CH2:4].[NH2:8][C@H:9]([C:17]([OH:19])=[O:18])[CH2:10][CH2:11][CH2:12][NH:13][C:14](=[NH:16])[NH2:15]>O>[C:2]([NH2:7])(=[O:6])[C:3]([CH3:5])=[CH2:4].[NH2:8][C@H:9]([C:17]([OH:19])=[O:18])[CH2:10][CH2:11][CH2:12][NH:13][C:14](=[NH:15])[NH2:16]

参加物

3

反応物 1

HCID 178449946HCID 178449946、化合物

生成物 1

HCID 178449950HCID 178449950、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

The obtained arginine-mono-methacrylamide hydrochloride(4.84 g) was dissolved in 40 ml of distilled water, and bubbled with nitrogen gas for 1 hour. Potassium persulfate(60 mg) was added to the solution, and dissolved in it. The reaction mixture was refluxed by heating for 3 hours, then cooled to room temperature, and poured into acetone, so that precipitates were deposited. The supernatant was discarded, and acetone was again added to the precipitates and obtained mixture was stirred. The deposition was collected by filtration and dried to obtain the target polymer (white powder, 3.05 g).

後処理

  1. custombubbled with nitrogen gas for 1 hour
  2. additionPotassium persulfate(60 mg) was added to the solution
  3. dissolutiondissolved in it
  4. temperatureThe reaction mixture was refluxed
  5. temperatureby heating for 3 hours
  6. additionpoured into acetone
  7. customso that precipitates
  8. additionacetone was again added to the
  9. customprecipitates
  10. customobtained mixture
  11. filtrationThe deposition was collected by filtration
  12. customdried
  13. customto obtain the target polymer (white powder, 3.05 g)

出典と根拠

ORDレコード
ord-6efe0540645444a58e5093ab19d41145
出典データセット
uspto-grants-2004_03
特許番号
US06703468B1

反応ノート

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