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Methanol → 4-Styrenesulfonic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | 2-Aminobenzenesulfonic acid | HCID 6926 | — |
| 反応物 | Sulfanilic acid | HCID 8479 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | 4-Styrenesulfonic acid | HCID 75905 | 73% |
反応手順
Example 13 was repeated, but instead of aniline-2-sulphonic acid the same amount of aniline-4-sulphonic acid and instead of methanol the same volume of iso-propanol were used. 15.0 g (73%) of styrene-4-sulphonic acid, Na salt, were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05231223 |
| 出典データセット | uspto-grants-1993_07 |
| ORD ID | ord-e2c419c1900c4b19bf38dbe1babbbe43 |
| 出典メモ | uspto-grants-1993_07 |