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HRID 484787作成日:2026年10月25日

2,6-Dimethyl-4-nitroaniline → 2-[(2,6-Dimethyl-4-nitrophenyl)amino]-1-pyrroline

https://huagongshe.com/reaction/484787

反応式

関与物質

役割名称HCID仕込み量
反応物2,6-Dimethyl-4-nitroanilineHCID 28159—
反応物2-Chloro-1-pyrrolineHCID 13520141—
生成物2-[(2,6-Dimethyl-4-nitrophenyl)amino]-1-pyrrolineHCID 20272394—

反応手順

A mixture of 2-chloro-1-pyrroline, prepared as in Example 1, and 19.9 g (0.12 mole) of the aniline product of Example 6 were heated at reflux overnight, according to the general method of Example 8. The title compound was isolated and used for subsequent reactions without further purification. Structure assignment was supported by nmr and infrared spectra.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04533739
出典データセットuspto-grants-1985_08
ORD IDord-b73808b27f264206b52ae5c5d7b1945f
出典メモuspto-grants-1985_08