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2,6-Dimethyl-4-nitroaniline → 2-[(2,6-Dimethyl-4-nitrophenyl)amino]-1-pyrroline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Dimethyl-4-nitroaniline | HCID 28159 | — |
| 反応物 | 2-Chloro-1-pyrroline | HCID 13520141 | — |
| 生成物 | 2-[(2,6-Dimethyl-4-nitrophenyl)amino]-1-pyrroline | HCID 20272394 | — |
反応手順
A mixture of 2-chloro-1-pyrroline, prepared as in Example 1, and 19.9 g (0.12 mole) of the aniline product of Example 6 were heated at reflux overnight, according to the general method of Example 8. The title compound was isolated and used for subsequent reactions without further purification. Structure assignment was supported by nmr and infrared spectra.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04533739 |
| 出典データセット | uspto-grants-1985_08 |
| ORD ID | ord-b73808b27f264206b52ae5c5d7b1945f |
| 出典メモ | uspto-grants-1985_08 |