化工社化工社 化学情報印刷レポート · 研究参考用
Carbon Dioxide → Ethyl 2-bromo-3-phenylpropanoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Carbon Dioxide | HCID 280 | — |
| 反応物 | Ethyl bromo-(phenylmethyl)propanedioate | HCID 86007639 | — |
| 生成物 | Ethyl 2-bromo-3-phenylpropanoate | HCID 4737529 | — |
反応手順
Ethyl bromo-(phenylmethyl)propandioate (XXVI, Example 60, 130 g.) is heated under reduced pressure to 140° with vigorous evolution of carbon dioxide. When decarboxylation is complete (about 5 minutes), the mixture is distilled to give ethyl 2-bromo-3-phenylpropionate, b.p. 120°/30 mm.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04534897 |
| 出典データセット | uspto-grants-1985_08 |
| ORD ID | ord-105355d6d3dc4bf48e8128d58f3d322d |
| 出典メモ | uspto-grants-1985_08 |