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Potassium Iodide → N-[[4-bromo-3-[1-(diallylcarbamoyl)ethoxy]phenyl]]-3,4,5,6-tetrahydrophthalimide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Iodide | HCID 4875 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | N-(4-bromo-3-hydroxyphenyl)-3,4,5,6-tetrahydrophthalimide | HCID 12769237 | — |
| 反応物 | N,N-diallyl alpha-bromopropionamide | HCID 13036601 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | N-[[4-bromo-3-[1-(diallylcarbamoyl)ethoxy]phenyl]]-3,4,5,6-tetrahydrophthalimide | HCID 13503503 | — |
反応手順
The reaction mixture was washed with water and dried and the solvent was distilled off to obtain 3.8 g. of N,N-diallyl α-bromopropionamide. The product was admixed with 3.5 g. of N-(4-bromo-3-hydroxyphenyl)-3,4,5,6-tetrahydrophthalimide, 2.2 g. of potassium carbonate, 1.8 g. of potassium iodide and 50 ml. of acetone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04536209 |
| 出典データセット | uspto-grants-1985_08 |
| ORD ID | ord-bf2d6795dd0b49899e460acfaecd3e6b |
| 出典メモ | uspto-grants-1985_08 |