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HRID 485299作成日:2026年10月24日

4-Toluenesulfonyl chloride → HCID 13957272、化合物

https://huagongshe.com/ja/reaction/485299

反応式

関与物質

役割名称HCID仕込み量
反応物4-Toluenesulfonyl chlorideHCID 7397—
反応物1-Octanol, 8-chloro-HCID 90012—
溶媒PyridineHCID 1049—
生成物HCID 13957272HCID 13957272—

反応手順

p-Toluenesulphonyl chloride (20.5 g) was added to a mixture of 8-chloro-1-octanol (17.7 g) and pyridine (50 ml) of 0°. After a hour the solution was added to ice and the mixture was extracted with ether. The ethereal solution was washed with dilute hydrochloric acid, dried with magnesium sulfate, and evaporated to yield the title compound as an oil.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04536503
出典データセットuspto-grants-1985_08
ORD IDord-b240b72b7cec4533bb47620064d06262
出典メモuspto-grants-1985_08