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4-Toluenesulfonyl chloride → HCID 13957272、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| 反応物 | 1-Octanol, 8-chloro- | HCID 90012 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | HCID 13957272 | HCID 13957272 | — |
反応手順
p-Toluenesulphonyl chloride (20.5 g) was added to a mixture of 8-chloro-1-octanol (17.7 g) and pyridine (50 ml) of 0°. After a hour the solution was added to ice and the mixture was extracted with ether. The ethereal solution was washed with dilute hydrochloric acid, dried with magnesium sulfate, and evaporated to yield the title compound as an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04536503 |
| 出典データセット | uspto-grants-1985_08 |
| ORD ID | ord-b240b72b7cec4533bb47620064d06262 |
| 出典メモ | uspto-grants-1985_08 |