Dimethylamine → 2-[2-(Dimethylamino)ethyl]-2,3-dihydro-4-methyl-1,4-oxazepino[6,7-h]quinoline-5(4H)-thione hydrochloride

HRID 4859ノート

反応式

HRID 4859 の反応式
[Cl:1][CH2:2][CH2:3][CH:4]1[CH2:18][N:17]([CH3:19])[C:16](=[S:20])[C:7]2[CH:8]=[CH:9][C:10]3[CH:11]=[CH:12][CH:13]=[N:14][C:15]=3[C:6]=2[O:5]1.[CH3:21][NH:22][CH3:23]>>[ClH:1].[CH3:21][N:22]([CH3:23])[CH2:2][CH2:3][CH:4]1[CH2:18][N:17]([CH3:19])[C:16](=[S:20])[C:7]2[CH:8]=[CH:9][C:10]3[CH:11]=[CH:12][CH:13]=[N:14][C:15]=3[C:6]=2[O:5]1

参加物

3

反応物 2

HCID 674DimethylamineHCID 212715722-(2-chloroethyl)-2,3-dihydro-4-methyl-1,4-oxazepino[6,7-h]quinoline-5(4H)-thione

生成物 1

HCID 212715642-[2-(Dimethylamino)ethyl]-2,3-dihydro-4-methyl-1,4-oxazepino[6,7-h]quinoline-5(4H)-thione hydrochloride

実験手順

Following the procedure of Example 31, 2-(2-chloroethyl)-2,3-dihydro-4-methyl-1,4-oxazepino[6,7-h]quinoline-5(4H)-thione is reacted with dimethylamine to give the title compound.

出典と根拠

ORDレコード
ord-c507885de2b74b8cbebd94b7d36d5089
出典データセット
uspto-grants-1988_02
特許番号
US04727152

反応ノート

読み込み中…