HCID 178445572、化合物 → HCID 178445571、化合物

反応式

[NH2:1][C:2]1[N:6]=[C:5]([S:7][CH2:8][CH2:9][S:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])[NH:4][N:3]=1.C(SCCSCCSC1N=C2N(N=1)[C:36]([OH:39])=[CH:35][C:34]([CH3:40])=N2)CCCCC>>[CH2:11]([S:10][CH2:9][CH2:8][S:7][C:5]1[N:6]=[C:2]2[N:3]([N:4]=1)[C:36]([OH:39])=[CH:35][C:34]([CH3:40])=[N:1]2)[CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

参加物

反応物 2

HCID 178445572HCID 178445572、化合物

HCID 178445573HCID 178445573、化合物

生成物 1

HCID 178445571HCID 178445571、化合物

実験手順

Compound 13 was prepared from Compound 6, using a procedure analogous to that described previously for Compound 20. The crude product was recrystallized from ethyl acetate to give a white solid, m.p. 125.5°-126° C. Analysis: Calculated for C14H22N4OS2 : C, 51.50; H, 6.79; N, 17.16. Found: C, 50.87; H, 6.62; N, 17.04.

後処理

customThe crude product was recrystallized from ethyl acetate
customto give a white solid, m.p. 125.5°-126° C

出典と根拠

ORDレコード: ord-361cb427744f454f9c7264dd2fa4270d
出典データセット: uspto-grants-1994_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05292627

反応ノート

読み込み中…

参加物