HCID 178443886、化合物 → HCID 178443885、化合物
反応式
[NH2:1][C:2]1[N:6]=[C:5]([S:7][CH2:8][CH2:9][S:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])[NH:4][N:3]=1.C(SCCSCCSC1N=C2N(N=1)[C:38]([OH:41])=[CH:37][C:36]([CH3:42])=N2)CCCCC>>[CH2:11]([S:10][CH2:9][CH2:8][S:7][C:5]1[N:6]=[C:2]2[N:3]([N:4]=1)[C:38]([OH:41])=[CH:37][C:36]([CH3:42])=[N:1]2)[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]参加物
3
実験手順
Compound 14 was prepared from Compound 7 using a procedure analogous to that described previously for Compound 20. Recrystallization of the crude product from ethyl acetate gave a 59% yield of a white solid, m.p. 125.5°-127° C. Analysis: Calculated for C16H26N4OS2 : C, 54.21; H, 7.39; N, 15.80. Found: C, 53.51; H, 7.21; N, 15.72.
後処理
- customRecrystallization of the crude product from ethyl acetate
出典と根拠
- ORDレコード
- ord-89aa3affed574ffe89719c32f51bd098
- 出典データセット
- uspto-grants-1994_03