関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydroquinone | HCID 785 | — |
| 反応物 | 2-Acryloxyethyl phthalate | HCID 22182166 | — |
| 反応物 | 2-Ethyl-2-(hydroxymethyl)propane-1,3-diol;prop-2-enoic acid | HCID 25019176 | — |
| 溶媒 | Dimethyl Phthalate | HCID 8554 | — |
| 生成物 | 2,2-Dimethoxy-2-phenylacetophenone | HCID 90571 | 472.6% |
反応手順
Isotactic polymethyl methacrylate (1.0 g), syndiotactic polymethyl methacrylate (3.0 g) and hydroquinone (0.03 g) were dissolved in a mixture of dimethyl phthalate (6.81 g), trimethylolpropane triacrylate (1.59 g) and HOA-MPL 2-acryloxyethyl phthalate (14.30 g), a product from Kyoeisha Oil and Fats K.K.) and heated to 120° C. After a clear sol was obtained 2,2-dimethyloxy-2-phenyl acetophenone (0.33 g) was added to the sol. The sol thus obtained was cast onto a 50 μm-thick polyester sheet and cooled at -5° C. for one hour to give a photocurable self-retainable gelled sheet having a thickness of 5 mm.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05292618 |
|---|
| 出典データセット | uspto-grants-1994_03 |
|---|
| ORD ID | ord-3bb98cc8f3734743b6f208817356c27e |
|---|
| 出典メモ | uspto-grants-1994_03 |
|---|
