化工社化工社 化学情報印刷レポート · 研究参考用
Trichloromethylsilane → HCID 131718361、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trichloromethylsilane | HCID 6399 | — |
| 反応物 | Neophyl chloride | HCID 68191 | — |
| 反応物 | Magnesium | HCID 5462224 | — |
| 反応物 | HCID 178418740 | HCID 178418740 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | HCID 131718361 | HCID 131718361 | 65% |
反応手順
In accord with the procedure of Example 1, neophylmagnesium chloride was prepared from 674 g (4 mol) of neophyl chloride and 105 g (4.4 mol) of magnesium turnings in 1.5 liters of dry THF. The neophylmagnesium chloride was added to 598 g (4 mol) of methyltrichlorosilane and 2 g of cuprous cyanide in 500 ml of THF. 640 g (65% of theory) of neophylmethyldichlorosilane was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05296624 |
| 出典データセット | uspto-grants-1994_03 |
| ORD ID | ord-c8ea5e0ccad847beb6efceb6b6122ccd |
| 出典メモ | uspto-grants-1994_03 |