化工社化工社 化学情報印刷レポート · 研究参考用
2-Oxo-1,3-thiazolidine-4-carboxylic acid → N-(3-Nitrooxypropyl)-2-oxothiazolidine-4-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Oxo-1,3-thiazolidine-4-carboxylic acid | HCID 65272 | — |
| 反応物 | 3-Nitroxypropylamine nitrate | HCID 22014591 | — |
| 生成物 | N-(3-Nitrooxypropyl)-2-oxothiazolidine-4-carboxamide | HCID 18961065 | 35.4% |
反応手順
A procedure similar to that described in Example 1 was repeated, but using 1.25 g of N-(3-nitrooxypropyl)-amine nitrate and 1.0 g of 2-oxothiazolidine-4-carboxylic acid, to obtain 0.60 g of the title compound as pale yellow crystals, melting at 83°-85° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05298516 |
| 出典データセット | uspto-grants-1994_03 |
| ORD ID | ord-b86c1d8036bc43feb049a8b38b5ce394 |
| 出典メモ | uspto-grants-1994_03 |