化工社化工社 化学情報印刷レポート · 研究参考用
Procysteine → (4R)-N-[1-(Nitrooxymethyl)ethyl]-2-oxothiazolidine-4-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Procysteine | HCID 72390 | — |
| 反応物 | 1-(Nitrooxymethyl)ethylamine nitrate | HCID 86747700 | — |
| 生成物 | (4R)-N-[1-(Nitrooxymethyl)ethyl]-2-oxothiazolidine-4-carboxamide | HCID 53804780 | — |
反応手順
A procedure similar to that described in Example 1 was repeated, but using 1.5 g of (4R)-2-oxothiazolidine-4-carboxylic acid and 2.3 g of 1-(nitrooxymethyl)ethylamine nitrate, to obtain 0.35 g of the title compound as colorless crystals, melting at 112°-114° C. (after recrystallization from ethanol).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05298516 |
| 出典データセット | uspto-grants-1994_03 |
| ORD ID | ord-e67d54e767a34183b3568da571737d4b |
| 出典メモ | uspto-grants-1994_03 |