4-Ethynyl-1,1'-biphenyl → 2-Biphenyl-4-ylethynyl-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester

HRID 488472

反応式

HRID 488472 の反応式
[CH2:1]([O:3][C:4]([C:6]1[N:7]([CH3:13])[C:8](Br)=[N:9][C:10]=1[CH3:11])=[O:5])[CH3:2].[C:14]([C:16]1[CH:21]=[CH:20][C:19]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)=[CH:18][CH:17]=1)#[CH:15]>>[CH2:1]([O:3][C:4]([C:6]1[N:7]([CH3:13])[C:8]([C:15]#[C:14][C:16]2[CH:21]=[CH:20][C:19]([C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)=[CH:18][CH:17]=2)=[N:9][C:10]=1[CH3:11])=[O:5])[CH3:2]

参加物

3

反応物 2

HCID 344644-Ethynyl-1,1'-biphenylHCID 13897513ethyl 2-bromo-1,4-dimethyl-1H-imidazole-5-carboxylate

生成物 1

HCID 99027122-Biphenyl-4-ylethynyl-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester

実験手順

The title compound, MS: m/e=345.4 (M+H+) was prepared in accordance with the general method of example 1b from 2-bromo-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester and 4-ethynylbiphenyl.

出典と根拠

ORDレコード
ord-4da7d1ce6a3740339c0c0cec90ed760f
出典データセット
uspto-grants-2005_12
特許番号
US06972299B2

関連ノート

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