化工社化工社 化学情報印刷レポート · 研究参考用
2-Ethylhexanoylbenzene → 2-Ethylhexylbenzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Ethylhexanoylbenzene | HCID 22269466 | — |
| 反応物 | HCID 178418361 | HCID 178418361 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | 2-Ethylhexylbenzene | HCID 22117015 | — |
反応手順
A solution of 313.9 grams of 2-ethylhexanoylbenzene in 500 mL of acetic acid with 11.4 grams of 10% palladium on carbon (as a catalyst) was stirred at 110° C. in an atmosphere of hydrogen at 414 kPa for 34 hours. The mixture was filtered through Celite™ diatomaceous earth filter agent to remove the catalyst. The filtrate was concentrated in vacuo to give 2-ethylhexylbenzene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06974877B2 |
| 出典データセット | uspto-grants-2005_12 |
| ORD ID | ord-75fd41b2bb1c4c978825c94bdee1aca0 |
| 出典メモ | uspto-grants-2005_12 |