関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Aluminum sec-butoxide | HCID 61289 | — |
| 反応物 | 3,10-Dihexylpentacene-5,12-dione | HCID 22269484 | — |
| 溶媒 | Cyclohexanol | HCID 7966 | — |
| 生成物 | 2,9-Dihexylpentacene | HCID 17973372 | — |
反応手順
A mixture of 5.69 grams of aluminum tri(sec-butoxide) and 49.1 mLs of cyclohexanol was made. To this was added 2.21 grams 3,10-Dihexylpentacene-5,12-dione. The reaction mixture was heated to 145° C. for 24 hours. The mixture was cooled to room temperature and the solid isolated by centrifugation. The solid was stirred with 40 mLs of cyclohexanol and centrifuged two times. The solid was collected by filtration and washed with THF to give 2,9-dihexylpentacene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06974877B2 |
|---|
| 出典データセット | uspto-grants-2005_12 |
|---|
| ORD ID | ord-6f4cfd59a8d54b509d5f65523dcba468 |
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| 出典メモ | uspto-grants-2005_12 |
|---|
