関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Aluminum sec-butoxide | HCID 61289 | — |
| 反応物 | 3,10-Dihexylpentacene-5,12-dione | HCID 22269484 | — |
| 溶媒 | Mesitylene | HCID 7947 | — |
| 生成物 | 2,9-Dihexylpentacene | HCID 17973372 | — |
反応手順
A mixture of 1.0 grams of 3,10-dihexylpentacene-5,12-dione and 2.5 grams of aluminum tri(sec-butoxide) in 50 mL of mesitylene was heated to 155° C. for 2 days and cooled. The reaction mixture was filtered and the residue washed with concentrated HCl to give 2,9-dihexylpentacene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06974877B2 |
|---|
| 出典データセット | uspto-grants-2005_12 |
|---|
| ORD ID | ord-2c8db88bb45447ab8ec829bde259eb2e |
|---|
| 出典メモ | uspto-grants-2005_12 |
|---|
