Methylamine → 3-Hydroxy-N-methyl-5-(trifluoromethyl)benzamide

反応式

[OH:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([C:11]([F:14])([F:13])[F:12])[CH:10]=1)[C:5](O)=[O:6].[CH3:15][NH2:16]>>[OH:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([C:11]([F:14])([F:13])[F:12])[CH:10]=1)[C:5]([NH:16][CH3:15])=[O:6]

参加物

反応物 2

HCID 6329Methylamine

HCID 27831463-hydroxy-5-(trifluoromethyl)benzoic Acid

生成物 1

HCID 674156453-Hydroxy-N-methyl-5-(trifluoromethyl)benzamide

実験手順

Prepared from 3-hydroxy-5-(trifluoromethyl)benzoic acid and methylamine using the method of preparation 58 to give the title compound as a pale orange solid.

後処理

customthe method of preparation 58

出典と根拠

ORDレコード: ord-dd04eb98f64542099fa59a8aaf4dd0ec
出典データセット: uspto-grants-2009_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07528170B2

反応ノート

読み込み中…