化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Methyl 4-Iodophenylacetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | 4-Iodophenylacetic acid | HCID 137214 | — |
| 溶媒 | 1,4-Dioxane | HCID 31275 | — |
| 生成物 | Methyl 4-Iodophenylacetate | HCID 10378700 | 98% |
反応手順
To a stirred solution of 4-iodophenylacetic acid (5.0 g, 19.1 mmol) in MeOH (200 mL) was added 4N hydrochloric acid in dioxane (10 mL). The reaction mixture was stirred for 24 h at room temperature and then the solvent was removed under reduced pressure to give the title compound (5.17 g, 98% yield), which was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07528253B2 |
| 出典データセット | uspto-grants-2009_05 |
| ORD ID | ord-15ce9d6f095f4c6ebd484d396d6f8dd3 |
| 出典メモ | uspto-grants-2009_05 |