化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl Bromide → Diethyl 3-Bromobenzylphosphonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl Bromide | HCID 6332 | — |
| 反応物 | Triethyl phosphite | HCID 31215 | — |
| 反応物 | 3-Bromobenzyl bromide | HCID 69979 | — |
| 生成物 | Diethyl 3-Bromobenzylphosphonate | HCID 10979718 | — |
反応手順
50 g (0.2 mol) of 3-bromobenzyl bromide and 33.2 g (0.2 mol) of triethyl phosphite were heated at 140° C. for 2 hours, during which ethyl bromide was distilled off. The product was distilled over a 30 cm Vigreux column.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05242908 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-5f68bfe24502413aa07932d4095cc464 |
| 出典メモ | uspto-grants-1993_09 |