化工社化工社 化学情報印刷レポート · 研究参考用
o-Xylyl bromide → Diisopropyl 2-methylbenzylphosphonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | o-Xylyl bromide | HCID 6992 | — |
| 反応物 | Triisopropyl phosphite | HCID 8304 | — |
| 生成物 | Diisopropyl 2-methylbenzylphosphonate | HCID 15166402 | — |
反応手順
34.5 g (0.19 mol) of 2-methylbenzyl bromide and 39 g (0.19 mol) of triisopropyl phosphite were heated at 150° C. for 2 hours. During this procedure, i-propyl bromide distilled off. The product was distilled through a 30 cm Vigreux column.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05242908 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-9bbd528effc4400bb7abc75186c3da13 |
| 出典メモ | uspto-grants-1993_09 |