化工社化工社 化学情報印刷レポート · 研究参考用
Azobisisobutyronitrile → Methyl 3-(bromomethyl)benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Azobisisobutyronitrile | HCID 6547 | — |
| 反応物 | Benzoic acid, 3-methyl-, methyl ester | HCID 7435 | — |
| 反応物 | N-bromobutanimide | HCID 67184 | — |
| 生成物 | Methyl 3-(bromomethyl)benzoate | HCID 517981 | — |
反応手順
Methyl m-toluate was brominated with NBS and AIBN as described in Example 21 to give methyl m-bromomethylbenzoate, and this was further reacted with triethyl phosphite as described in Example 2 without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05242908 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-72cd4b260c0043e8aa2503a92dce1f5e |
| 出典メモ | uspto-grants-1993_09 |