化工社化工社 化学情報印刷レポート · 研究参考用
Azobisisobutyronitrile → Ethyl o-bromomethylphenylacetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Azobisisobutyronitrile | HCID 6547 | — |
| 反応物 | N-bromobutanimide | HCID 67184 | — |
| 反応物 | o-Tolylacetic acid | HCID 69519 | — |
| 生成物 | Ethyl o-bromomethylphenylacetate | HCID 13052926 | — |
反応手順
o-Tolylacetic acid was brominated with NBS and AIBN as described in Example 21 to give ethyl o-bromomethylphenylacetate, and this was reacted with triethyl phosphite as described in Example 2.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05242908 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-67807ba4f6aa49a6bfa5666d55bc49c7 |
| 出典メモ | uspto-grants-1993_09 |