化工社化工社 化学情報印刷レポート · 研究参考用
1,8,8-Trimethyl-3-oxabicyclo[3.2.1]octane-2,4-dione → HCID 10408650、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,8,8-Trimethyl-3-oxabicyclo[3.2.1]octane-2,4-dione | HCID 94834 | — |
| 反応物 | 4-(2-Pyrimidinyl)-1-piperazinebutanamine | HCID 12840705 | — |
| 生成物 | HCID 10408650 | HCID 10408650 | 17% |
反応手順
The title compound was prepared from 2.47 g (10.4 mmol) of 1-(4-aminobutyl)-4-(2-pyrimidinyl)piperazine and 1.89 g (10.3 mmol) of dl-camphoric anhydride, substantially according to the procedure of Example 1. This afforded 0.7 g of product, mp 94°-97° C. (17% yield).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05242911 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-88cb2fb8067f482b8c767b3656f1557f |
| 出典メモ | uspto-grants-1993_09 |