関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Phenylphosphonic Acid | HCID 15295 | — |
| 反応物 | Magnesium Hydroxide | HCID 73981 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 21506410 | HCID 21506410 | 99% |
反応手順
1.58 g (10.0 mmol) of phenylphosphonic acid (manufactured by Nissan Chemical industries, Ltd.), 0.583 g (10.0 mmol) of magnesium hydroxide and 41 g of water were mixed, stirred at 80° C. for 3 hours, then water was distilled off under reduced pressure and dried at 200° C. to obtain 1.78 g (yield 99%) of the aimed product as white crystal. Decomposition temperature: 524° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07531585B2 |
|---|
| 出典データセット | uspto-grants-2009_05 |
|---|
| ORD ID | ord-c57a87bc93e14e7fbbb1c2c9a1a8f65f |
|---|
| 出典メモ | uspto-grants-2009_05 |
|---|
