化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → Disodium phenylphosphonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Phenylphosphonic Acid | HCID 15295 | — |
| 生成物 | Disodium phenylphosphonate | HCID 12499978 | 176.2% |
反応手順
In 1.58 g (10.0 mmol) of phenylphosphonic acid (manufactured by Nissan Chemical industries, Ltd.), 20 mL (10.0 mmol) of 0.5 N sodium hydroxide was added, stirred at room temperature for 10 minutes, then water was distilled off under reduced pressure and dried to obtain 1.78 g (yield 99%) of the aimed product as white crystal. Decomposition temperature: 480° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07531585B2 |
| 出典データセット | uspto-grants-2009_05 |
| ORD ID | ord-d3045a8b377a4668b55573e090b8f1c1 |
| 出典メモ | uspto-grants-2009_05 |