化工社化工社 化学情報印刷レポート · 研究参考用
1-Pentyne → 2-(Benzyloxy)-6-(2-n-propylethynyl)naphthalene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Pentyne | HCID 12309 | — |
| 反応物 | Trimethylsilylacetylene | HCID 66111 | — |
| 反応物 | 2-(Benzyloxy)-6-bromonaphthalene | HCID 640595 | — |
| 生成物 | 2-(Benzyloxy)-6-(2-n-propylethynyl)naphthalene | HCID 22925806 | — |
反応手順
The reaction was conducted in the same manner as in the step (i) of the Example 31, except for using 2-(benzyloxy)-6-bromonaphthalene synthesized in the step (i) and 1-n-pentyne instead of 1-bromo-4-n-propylbenzene and trimethylsilylacetylene, respectively. The resultant was recrystallized from ethanol to give 2-(benzyloxy)-6-(2-n-propylethynyl)naphthalene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07534547B2 |
| 出典データセット | uspto-grants-2009_05 |
| ORD ID | ord-5f136b0ba30b4f178ad1f7d0f9a890a6 |
| 出典メモ | uspto-grants-2009_05 |