化工社化工社 化学情報印刷レポート · 研究参考用
1,2-Benzenedicarboxylic acid, 4-nitro- → 4-Aminophthalic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Benzenedicarboxylic acid, 4-nitro- | HCID 69121 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 4-Aminophthalic acid | HCID 72912 | — |
反応手順
1 g (4.73 mmol) of 4-nitrophthalic acid is dissolved in 10 mL of anhydrous ethanol. The solution is stirred at room temperature and degassed under argon. 50 mg of palladium/charcoal (5%) are added in a single portion and hydrogen is bubbled into the solution. After 3 hours, the solution is filtered through Celite and then evaporated.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06706725B1 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-d56bdbc58160413788ea7d8ded70198f |
| 出典メモ | uspto-grants-2004_03 |