化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → 4-Ethoxycarbonylphenylboronic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 4-Carboxyphenylboronic Acid | HCID 312183 | — |
| 生成物 | 4-Ethoxycarbonylphenylboronic acid | HCID 2734350 | — |
反応手順
A solution of 4-carboxyphenylboronic acid (15 g, 0.09 mol), 99% ethanol (150 mL) and concentrated sulphuric acid (0.5 mL) was heated to reflux for two days. The volume was reduced to approximately 20 mL. The residue was triturated with petroleum ether to give 13.4 g of the desired material.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06706749B2 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-bf48985882e84c38afed626b7b44b7a8 |
| 出典メモ | uspto-grants-2004_03 |