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1,5-Dibromopentane → 6-(5-Bromo-pentyloxy)-3,4-dihydro-2H-quinoline-1-carboxylic acid tert-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,5-Dibromopentane | HCID 8100 | — |
| 反応物 | Tert-butyl 6-hydroxy-3,4-dihydroquinoline-1(2H)-carboxylate | HCID 53408427 | — |
| 生成物 | 6-(5-Bromo-pentyloxy)-3,4-dihydro-2H-quinoline-1-carboxylic acid tert-butyl ester | HCID 69514902 | 63% |
反応手順
In analogy to example 2.2, 6-Hydroxy-3,4-dihydro-2H-quinoline-1-carboxylic acid tert-butyl ester and 1,5-dibromopentane were converted to yield 6-(5-Bromo-pentyloxy)-3,4-dihydro-2H-quinoline-1-carboxylic acid tert-butyl ester (63%) as colorless oil, MS: 397 (M, 1Br);
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06706751B2 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-3ccff50af97f4bf7a926d30851c2e665 |
| 出典メモ | uspto-grants-2004_03 |