化工社化工社 化学情報印刷レポート · 研究参考用
N-(2-Methoxyethyl)ethylamine → 5-{4-[(2-Methoxy-ethyl)-methyl-amino]-butoxy}-2,3-dihydro-indole-1-carboxylic acid tert-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-(2-Methoxyethyl)ethylamine | HCID 546877 | — |
| 反応物 | 5-(4-Bromo-butoxy)-2,3-dihydro-indole-1-carboxylic acid tert-butyl ester | HCID 69514776 | — |
| 生成物 | 5-{4-[(2-Methoxy-ethyl)-methyl-amino]-butoxy}-2,3-dihydro-indole-1-carboxylic acid tert-butyl ester | HCID 69514492 | — |
反応手順
In analogy to example 7.2, 5-(4-Bromo-butoxy)-2,3-dihydro-indole-1-carboxylic acid tert-butyl ester and methoxyethyl-ethylamine were converted to yield 5-{4-[(2-Methoxy-ethyl)-methyl-amino]-butoxy}-2,3-dihydro-indole-1-carboxylic acid tert-butyl ester as colorless oil, MS: 379 (MH+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06706751B2 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-a30536b2cdbc41fa876b13256e605af7 |
| 出典メモ | uspto-grants-2004_03 |