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2-(Benzyloxy)-6-butylpyridine → 6-Butylpyridin-2-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(Benzyloxy)-6-butylpyridine | HCID 66626481 | — |
| 反応物 | HCID 178418361 | HCID 178418361 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 6-Butylpyridin-2-ol | HCID 23352100 | — |
反応手順
To a pressure reaction bottle were added 1.6 g 2-(benzyloxy)-6-butylpyridine, 0.2 g 5% palladium on carbon and 50 ml ethanol. The mixture was hydrogenated at 22 C and 40 psi hydrogen for 16 hours. Following filtration through celite and solvent removal, an oil was obtained that crystallized on standing to give 0.9 g.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07538931B2 |
| 出典データセット | uspto-grants-2009_05 |
| ORD ID | ord-9846a64eb1374f1db7869785d1743f74 |
| 出典メモ | uspto-grants-2009_05 |