化工社化工社 化学情報印刷レポート · 研究参考用
Formaldehyde → Melamine formaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formaldehyde | HCID 712 | — |
| 反応物 | Oxygen | HCID 977 | — |
| 反応物 | Melamine | HCID 7955 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Melamine formaldehyde | HCID 93374 | — |
反応手順
A melam-containing melamine-formaldehyde solution was prepared by dissolving 1113 g of multicrystalline melamine according to the invention (melam content=2 wt. %; oxygen-containing components=0.4 wt. %; specific surface area=1.3 m2/g; color=14 APHA) in 1589 g of a 30% formalin solution and 272 g water, the pH of which had been adjusted to 9.0 with 2 N NaOH, and then heating it to reflux temperature. After 87 minutes a water tolerance of 1.0 (g water/g resin) was reached. The water tolerance is the amount of water in gram that can be added at 20° C. to 1 g of resin before the resin turns turbid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06706856B2 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-ba4de474c8114313babfa6d59b514264 |
| 出典メモ | uspto-grants-2004_03 |