1,2-Dichloroethane → HCID 131716892、化合物

HRID 495960ノート

反応式

HRID 495960 の反応式
[CH2:1]([Cl:4])[CH2:2][Cl:3].[CH3:5][O:6][C:7](=[O:15])[C@H:8]([CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[NH2:9]>O>[CH2:1]([Cl:4])[CH2:2][Cl:3].[CH3:5][O:6][C:7](=[O:15])[C@H:8]([CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[NH2:9]

参加物

4

反応物 2

HCID 111,2-Dichloroethane4 回HCID 117779L-Lysine, methyl ester3 回

生成物 1

HCID 131716892HCID 131716892、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

A 0.4% (w/w) solution of HA in water was prepared. The pH of this solution was adjusted to between 4.3 and 4.75 by addition of acid. To each 100 ml of this solution was added 0.76 g of EDC with stirring until the EDC had completely dissolved. To each 100 ml of the HA/EDC solution was added 0.20 g of lysine methyl ester (LME) with stirring until the LME had completely dissolved. The addition of HA, EDC, and LME was conducted at room temperature; once the final HA/EDC/LME solution had been formed, it was stored at 4° C. until needed.

後処理

  1. additionThe pH of this solution was adjusted to between 4.3 and 4.75 by addition of acid
  2. dissolutionhad completely dissolved
  3. dissolutionhad completely dissolved
  4. customwas conducted at room temperature

出典と根拠

ORDレコード
ord-5a159504915f4894ad42a51bfd18ef87
出典データセット
uspto-grants-2005_09
特許番号
US06943154B2

反応ノート

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