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Hydrogen Bromide → 4-(Naphth-1-yl)piperidine hydrobromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrogen Bromide | HCID 260 | — |
| 反応物 | Ethyl [4-(naphth-1-yl)piperid-1-yl]carbamate | HCID 54406105 | — |
| 生成物 | 4-(Naphth-1-yl)piperidine hydrobromide | HCID 19096220 | 86.64% |
反応手順
10.5 g of the compound obtained in Stage A in 300 ml of a 48% hydrobromic acid solution, are refluxed for 20 hours. After evaporation and washing twice with ethanol, the residue is taken up in acetone and the mixture then filtered to give 4-(naphth-1-yl)piperidine hydrobromide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05242933 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-2b73ef6cf0d74456b104b1399812863b |
| 出典メモ | uspto-grants-1993_09 |