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Methyl Decanoate → Decanohydrazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl Decanoate | HCID 8050 | — |
| 反応物 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Decanohydrazide | HCID 98597 | 94% |
反応手順
17.5 g of decanoic acid methyl ester is dissolved in 1 l of absolute ethanol and mixed with 350 ml of hydrazine hydrate. It is refluxed for 3 hours and then stirred overnight at room temperature. The solution is concentrated by evaporation to about 300 ml and allowed to stand until the product is crystallized out. After it is filtered off and dried, 16.6 g (=94% of theory) of decanoic acid hydrazide is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06709693B1 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-d63e462b8fd14c8bbc6a3c4b6aae5b72 |
| 出典メモ | uspto-grants-2004_03 |