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2-Chloro-6-ethoxypyridine → HCID 22320216、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Chloro-6-ethoxypyridine | HCID 98563 | — |
| 反応物 | 8-methyl-2-(2-oxopropyl)-4H-3,1-benzoxazin-4-one | HCID 22320304 | — |
| 反応物 | 6-Ethoxy-2-hydrazinopyridine | HCID 22320339 | — |
| 生成物 | HCID 22320216 | HCID 22320216 | — |
反応手順
Following the procedures described in Reference Example 1-10 and Example 1-34, the title compound was prepared from 8-methyl-2-(2-oxopropyl)-4H-3,1-benzoxazin-4-one and 6-ethoxy-2-hydrazinopyridine which was separately prepared from 2-chloro-6-ethoxypyridine following the method described in Reference Example 1-9 (62% yield).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06949648B2 |
| 出典データセット | uspto-grants-2005_09 |
| ORD ID | ord-c77e31a31bb247c5b7e0952b3dfaa044 |
| 出典メモ | uspto-grants-2005_09 |