化工社化工社 化学情報印刷レポート · 研究参考用
2-Amino-3,3-dimethylbutanamide → (2R)-2-Amino-3,3-dimethylbutanamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-3,3-dimethylbutanamide | HCID 3496444 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | (2R)-2-Amino-3,3-dimethylbutanamide | HCID 10197708 | — |
反応手順
In accordance with the process described in JP Patent Application Laying Open (Kokai) No. 62-55097, Enterobacter cloacae N-7901 (FERM BP-873) was cultured. 1 L of culture solution was centrifuged, and the wet cells were then suspended in distilled water to prepare a 800 g cell suspension. 200 g of D,L-tert-leucine amide was dissolved in this suspension, and the solution was then allowed to react at 40° C. for 52 hours. After the reaction, cells were removed by centrifugation and 970 g of an aqueous solution containing 10% by mass each of L-tert-leucine and D-tert-leucine amide was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06949658B2 |
| 出典データセット | uspto-grants-2005_09 |
| ORD ID | ord-a6931ace804f4de0aea194ee160ea841 |
| 出典メモ | uspto-grants-2005_09 |