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HRID 498088作成日:2026年10月26日

2-Amino-3,3-dimethylbutanamide → (2R)-2-Amino-3,3-dimethylbutanamide

https://huagongshe.com/reaction/498088

反応式

関与物質

役割名称HCID仕込み量
反応物2-Amino-3,3-dimethylbutanamideHCID 3496444—
溶媒WaterHCID 962—
生成物(2R)-2-Amino-3,3-dimethylbutanamideHCID 10197708—

反応手順

In accordance with the process described in JP Patent Application Laying Open (Kokai) No. 62-55097, Enterobacter cloacae N-7901 (FERM BP-873) was cultured. 1 L of culture solution was centrifuged, and the wet cells were then suspended in distilled water to prepare a 800 g cell suspension. 200 g of D,L-tert-leucine amide was dissolved in this suspension, and the solution was then allowed to react at 40° C. for 52 hours. After the reaction, cells were removed by centrifugation and 970 g of an aqueous solution containing 10% by mass each of L-tert-leucine and D-tert-leucine amide was obtained.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06949658B2
出典データセットuspto-grants-2005_09
ORD IDord-a6931ace804f4de0aea194ee160ea841
出典メモuspto-grants-2005_09