化工社化工社 化学情報印刷レポート · 研究参考用
Phenylalanine amide → (2R)-2-amino-3-phenylpropanamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenylalanine amide | HCID 445694 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | (2R)-2-amino-3-phenylpropanamide | HCID 7000171 | — |
反応手順
In accordance with the process described in JP Patent Application Laying Open (Kokai) No. 62-55097, Enterobacter cloacae N-7901 (FERM BP-873) was cultured. This culture solution, 500 mL, was centrifuged, and the wet cells were then suspended in distilled water to prepare a 1,140 g cell suspension. D, L-phenylalanine amide, 60 g, was dissolved in this suspension, and the mixture was then allowed to react at 40° C. for 24 hours. After the reaction, cells were removed by centrifugation and 1,150 g of an aqueous solution containing 2.5% by mass each of L-phenylalanine and D-phenylalanine amide was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06949658B2 |
| 出典データセット | uspto-grants-2005_09 |
| ORD ID | ord-48e42abb38bb4bc8ad7561b1cc61f9b2 |
| 出典メモ | uspto-grants-2005_09 |